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Beilstein J. Org. Chem. 2015, 11, 2087–2096, doi:10.3762/bjoc.11.225
Graphical Abstract
Figure 1: Hoveyda–Grubbs type catalysts used for immobilization.
Scheme 1: RCM of (−)-β-citronellene (1) and N,N-diallyl-2,2,2-trifluoroacetamide (2).
Figure 2: Conversion vs time dependence for RCM of (−)-β-citronellene over HGIIN+Cl−/MCM-36 (●), HGIIN+Cl−/SB...
Figure 3: Conversion vs. time dependences for RCM of DAF over catalysts HGIIN+Cl−/MCM-22 (▲), HGIIN+Cl−/MCM-5...
Figure 4: Splitting test for HGIIN+Cl−/MCM-56 in RCM of (−)-β-citronellene. Toluene, 60 °C, molar ratio (−)-β...
Figure 5: Self-metathesis of methyl oleate over HGIIN+Cl−/SBA-15 (■), HGIIN+Cl−/MCM-22 (▲), HGIIN+Cl−/MCM-56 ...
Scheme 2: Cross-metathesis of methyl oleate with cis-3-hexenyl acetate.
Figure 6: Conversion curves for CM of methyl oleate (full symbols) with cis-3-hexenyl acetate (open symbols) ...